Calibration of pH Meter in Quality Assurance B.Pharmacy 6th Semester
CALIBRATION OF pH METER
B.PHARMACY 6
TH SEMESTER
SDPGIPS Rohtak
1 A pH meter is an electronic instrument used for measuring the
pH (acidity or alkalinity) of a liquid (though special probes are
sometimes used to measure the pH of semi-solid substances).
A typical pH meter consists of special measuring probes (a
glass electrode and a reference electrode) connected to an
electronic meter that measures and displays the pH reading.
INTRODUCTION
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2 pH is defined as the negative logarithm of hydrogen ion concentration.
pH= -log [ H+ ]
p = power
H = hydrogen
[H+ ] = hydrogen ion concentration
The pH of a solution can be measured by the pH meter. The glass electrode is an half cell and the
calomel electrode is another half cell.
PRINCIPLE
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3 WHAT IS CALIBRATION
Calibration is the act of ensuring that a method or
instrument used in measurement will produce accurate
results.
Calibration is performed using primary reference standard
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4 NEED OF CALIBRATION
When a specific time period is elapsed.
When a specific operating hours has elapsed.
With a new instrument.
When observations appear questionable.
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5 PARTS OF DIGITAL PH METER
pH electrode
Device have 4 knobs
6 FUNCTION MODE
Function Mode
pH Mode
(used to measure
pH by rotation)
Standby mode
MV Mode
(used to measure
mv)
• Temperature settling knob: To set temperature
• Calibration knob: rotate to adjust and set Ph value to standard pH value
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7 PROCEDURE
First of all, calibrate the pH meter. & prepare standard buffer solition of pH 4 and ph 7 (calibratin by standard
buffer solution of pH7)
First dip electrode in standard buffer solution of pH 7
Then set temperature at 25°c by rotating temperate knob.
Rotate the function knob to pH mode.
And wail for constant display reeding.
Rotate calibration Knob to the right display reading become 7.
Rotate function knob to standby mode and Remove electrode from solution
Then rinse electrode with distilled water and dry it with tissue paper.
SDPGIPS Rohtak
8 PROCEDURE
Calibrate the pH meter. & prepare standard buffer solution of pH 4 and pH 7 (calibration by standard buffer
solution of pH4)
First dip electrode in standard buffer solution of pH 4
Then set temperature at 25°c by rotating temperate knob.
Rotate the function knob to pH mode.
And wail for constant display reeding.
Rotate slope Knob to the right display reading become 4.
Rotate slope knob to standby mode and Remove electrode from solution
Then rinse electrode with distilled water and dry it with tissue paper.
SDPGIPS Rohtak
10
Thank you
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